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Common problems of rotary evaporator 500ml, 1L, 2L

Zhengzhou Greatwall Scientific Industrial and Trade Co.,Ltd
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Common problems of rotary evaporator 500ml, 1L, 2L

Place of Origin : China

Brand Name : Greatwall

Certification : ISO9001:2008

Model Number : R-1001VN, R-1001LN

MOQ : 1

Price : US $1,077 - 1,267 / Unit

Packaging Details : Carton box

Delivery Time : within 7 working days after receiving the payment

Payment Terms : T/T

Supply Ability : 300 sets/month

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Common failure and solutions of Zhengzhou Greatwall Rotary Evaporator 500ml,1L,2L

 


Situation

probable cause

Solutions

Instrument doesn’t work

Power is off

Open the power switch

Instrument do not connect the power supply

Check the connection of power supply

Water Bath does not heating

(heating light is off)

Settled temperature is improper

Change the settled temperature

Control pannel failure

Stop using it immediately and contact us(or our agents)

Water bath does not heating

(heating light is on)

Heater circuit break, or heater terminals fall off

Senser fall off

Temperature monitor displays ER2

Temperature feedback signal is wrong

Stop using it immediately and contact us(or our agents)

Rotation is disabled

Power supply is unnormal

Check the power supply

Rotary button turn to zero(0)

Rotate the rotary button clockwise until it is start rotating

system leakage

Each joint do not paint with grease

Lubricate each joint

Pipeline connection is not correct or pipe defect

Check the pipeline connection

Pipeline leak (brittle)

Change the pipeline

Sealing system installation is not correct

Check the sealing system

Sealing problem

Change the seal

 

Specifications:

1.ISO 9001:2008 Certification,one year warranty

2.Stainless steel water bath, temp.range:RT~99Celsius

3.PTFE sealing

Common problems of rotary evaporator 500ml, 1L, 2L

Brief introduction of 500ml,1L,2L Rotary Evaporator:

A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. Rotary evaporator is most often and conveniently applied to separate "low boiling" solvents such as n-hexane or ethyl acetate from compounds which are solid at room temperature and pressure. However, careful application also allows removal of a solvent from a sample containing a liquid compound if there is minimal co-evaporation (azeotropic behavior), and a sufficient difference in boiling points at the chosen temperature and reduced pressure.

 

The Zhengzhou Greatwall 500ml,1L,2L (evaporating flask capacity) series rotary evaporators come with a modular heating bath, vertical glassware, and digital temperature/rotation control, with optimized bath volume allows for fast heat-up times. The condenser unit has special designed glass tubes that utilize surface extremely efficient. That’s why our SolventVap delivers reliable and reproducible process results that are usually reserved for more costly systems. Another important aspect of the SolventVap are the safety features, including dry-run protection, water bath over-temp shut-off protection, and fuse protection.

Rotary evaporator features a specially designed motor and worm gear to provide constant rotation at speeds from 10 to 180 rpm. As the flask containing the solvent is rotated, it continually transfers a thin layer of liquid over the entire inner surface. This gives a very large surface area for evaporation that is effected by heating from the water bath. The rotating system is fitted with a special seal that allows the apparatus to be placed under vacuum. This reduces the boiling point of the solvents and removes the vapor phase making the process much more efficient. Each unit is also provided with an easy to use vacuum release and a continuous feed system, which allows more solvent to be drawn into the rotating flask without the need to stop the operation.

Digital water bath operates from ambient to 99°C (210°F) with PID temperature control stepping at 0.1°C. Heating coils are located directly inside the pan for the most efficient heating. Built-in overheat protector shuts down power in case of controller failure.

Standard Glassware Set 0.5L, 1L or 2 liters pear shaped evaporating flask, 1 liter round-bottomed receiving flask, and vertical condenser. Rotary evaporators with vertical glass condenser for are good for distillation of solvents with higher boiling points.

Features of 500ml,1L,2L Rotary Evaporator:

  • Solvent-resistant PTFE and Viton gaskets ensuring long time operation.
  • Specialized motor and extremely compact intermeshed worm and worm gear provide precise driving, for very quiet and vibration free operation.
  • Downward condenser vacuum connector design ensures safe vacuum operation.
  • Modular design (individual rotary and water bath modules) for easy future upgrade.
  • Operate visually and easily with digital speed and temperature display.
  • PID temperature controller for accurate and flexible temperature control.
  • One year warranty and life-long service support.

Specifications of 500ml,1L,2L Rotary Evaporator: 

 Electrical requirements

 110V 60Hz single phase, (heater: 1500 watts, rotation motor: 25 watts)

 Evaporating flask

 Capacity: 0.5L,1L or 2L
 Rotation speed: 10 to 180 rpm
 Evaporating speed: 20 ml per minute
 Lifting: weight balancing manual control with lock
 Max lifting distance: 100mm (extendable to 150mm)

 Receiving flask

 1 liter

 Water bath

Temperature range: ambient to 99° (210°F)
 Temperature controller: digital
 Capacity: 7.4L
 Material: stainless steel
 Dimensions: 10" diameter x 5" depth x 9.75" height
 Media: water
 Number of heaters: one

 Vacuum level

 < 3 torrs(399.9Pa)

 Vacuum sealing

 PTFE + Viton gaskets

 Safety

 Dry-run, over-temp shut-off, fuse protections

 

 

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